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1. Function of single crystal diffractometer: The TD-5000 X-ray single crystal diffractometer is mainly used to determine the three-dimensional spatial structure and electron cloud density of crystalline substances such as inorganic, organic, and metal complexes, and to analyze the structure of special materials such as twinning, non commensurate crystals, quasicrystals, etc. Determine the accurate three-dimensional space (including bond length, bond angle, configuration, conformation, and even bonding electron density) of new compound (crystalline) molecules and the actual arrangement of molecules in the lattice; X-ray single crystal diffractometer can provide information on the crystal cell parameters, space group, crystal molecular structure, intermolecular hydrogen bonding and weak interactions, as well as structural information such as molecular configuration and conformation.X-ray single crystal diffractometer is widely used in analytical research in chemical crystallography, molecular biology, pharmacology, mineralogy, and materials science. The X-ray single crystal diffractometer is a high-tech product funded by the Ministry of Science and Technology of China's National Major Scientific Instrument and Equipment Development Project, led by Dandong Tongda Technology Co., Ltd., filling the gap in the development and production of single crystal diffractometers in China. 2. Characteristics of single crystal diffractometer: The whole machine adopts programmable logic controller (PLC) control technology; Easy to operate, one click collection system; Modular design, plug and play accessories, no need for calibration; Real time online monitoring through touch screen, displaying instrument status; High power X-ray generator with stable and reliable performance; Electronic lead door interlocking device, dual protection. 3. Accuracy of single crystal diffractometer: 2 θ angle repeatability accuracy: 0.0001 °; Minimum step angle: 0.0001 ° Temperature control range: 100K-300K; Control accuracy: ± 0.3K 4. Angle measuring instrument used in single crystal diffractometer: The use of four concentric circles technique ensures that the center of the angle measuring instrument remains unchanged regardless of any rotation, achieving the goal of obtaining the most accurate data and obtaining higher completeness. Four concentric circles are a necessary condition for conventional single crystal diffractometer scanning. 5. High speed two-dimensional detector used in X-ray single crystal diffractometer: The detector combines the key technologies of single photon counting and mixed pixel technology to achieve the best data quality while ensuring low power consumption and low cooling. It is applied in various fields such as synchrotron radiation and conventional laboratory light sources, effectively eliminating the interference of readout noise and dark current. The mixed pixel technology can directly detect X-rays, make the signal easier to distinguish, and efficiently provide high-quality data. 6. Low temperature equipment used in X-ray single crystal diffractometer: The data collected through low-temperature equipment yields more ideal results. With the help of low-temperature equipment, more advantageous conditions can be provided to enable undesirable crystals to obtain ideal results, as well as ideal crystals to obtain more ideal results. Temperature control range: 100K~300K; Control accuracy: ± 0.3K; Liquid nitrogen consumption: 1.1~2 liters/hour; 7. Optional accessory, multi-layer film focusing lens: X-ray tube power: 30W or 50W, etc; Divergence: 0.5~1 mrad; X-ray tube target material: Mo/Cu target; Focal spot: 0.5~2mm.
The graphite curved crystal monochromator used in X-ray diffractometers is a key component for selecting specific wavelengths of X-rays and removing unwanted radiation such as K β lines and fluorescent X-rays. The graphite curved crystal monochromator is a component installed in front of the X-ray detector, which monochromatizes the X-rays passing through the receiving slit and only detects the Kα characteristic X-rays in the X-ray spectrum. By using this device, continuous X-rays, K β characteristic X-rays, and fluorescent X-rays can be completely eliminated, enabling high signal-to-noise ratio X-ray diffraction analysis. When copper target X-ray tubes are used in conjunction with corresponding monochromators, fluorescent X-rays generated from Mn, Fe, Co, Ni based samples can be eliminated, making them suitable for analysis of various samples. working principle: Bragg diffraction: Based on Bragg's law, when X-rays are incident on a crystal at a certain angle, if 2dsin θ=n λ (where d is the interplanar spacing of the crystal, θis the incident angle, λ is the wavelength of the X-ray, and n is an integer), diffraction will occur. It utilizes this principle to adjust the orientation of the crystal so that only X-rays that meet specific conditions can pass through, thereby achieving the selection of X-ray wavelengths. Energy resolution: Due to the interplanar spacing and structural characteristics of graphite crystals, it can effectively distinguish X-rays of different energies. High energy resolution graphite curved crystal monochromator can further reduce unwanted radiation and improve the quality of diffraction data. Structural features: Curved shape: graphite curved crystal monochromator typically have a curved shape, which helps focus X-rays and improve diffraction efficiency. At the same time, the curved shape also helps to reduce the stress on the crystal, improve its stability and service life. High purity graphite: Graphite curved crystal monochromator is usually made of high-purity graphite materials to ensure their good diffraction performance and stability. High diffraction efficiency: It has a high diffraction efficiency, which can effectively select X-rays of the desired wavelength, thereby improving the quality of diffraction data. Wide wavelength range: It can operate over a wide wavelength range and is suitable for various types of X-ray diffraction experiments. Good stability: Due to the use of high-purity graphite material, it has good stability and a long service life. Application areas: Materials Science: In the field of materials science, X-ray diffractometers are widely used to study the crystal structure, phase composition, and other properties of materials. The graphite curved crystal monochromator, as an important component of X-ray diffractometer, provides important technical support for materials science research. Physics: In the field of physics, X-ray diffractometers are also used to study the microstructure and physical properties of matter. In summary, the graphite curved crystal monochromator used in X-ray diffractometers is an efficient and accurate X-ray selection and filtering device, providing important technical support for X-ray diffraction experiments.
The X-ray crystal orienter operates based on the principle of X-ray diffraction. The high voltage generated by the high-voltage transformer acts on the X-ray tube, producing X-rays. When the X-ray is irradiated onto the sample, diffraction occurs when the Bragg diffraction condition (n λ=2dsin θ) is satisfied. Among them, λ is the wavelength of X-rays, d is the spacing between atomic planes inside the crystal, and θ is the angle between the incident X-rays and the crystal plane. The diffraction line is received by the counting tube and displayed on the microampere meter of the amplifier. When using a monochromator, the diffraction line is monochromatized and then received by the counter and displayed on the microampere meter of the amplifier, thereby improving measurement accuracy. The X-ray crystal orienter can accurately and quickly determine the cutting angle of natural and artificial single crystals (piezoelectric crystals, optical crystals, laser crystals, semiconductor crystals), and is equipped with a cutting machine for directional cutting of the above-mentioned crystals. X-ray crystal orienter is an indispensable instrument for precision machining and manufacturing of crystal devices. The X-ray crystal orienter is widely used in the research, processing, and manufacturing industries of crystal materials. The X-ray crystal orienter is easy to operate, does not require professional knowledge or skilled techniques, displays the angle digitally, is easy to observe, and reduces reading errors. The display of the X-ray crystal orientation instrument can be zeroed at any position, making it easy to display the deviation value of the chip angle. The dual angle measuring instrument can work simultaneously, improving efficiency. The X-ray crystal orienter has a special integrator with peak amplification, which improves the detection accuracy. The integration of X-ray tube and high-voltage cable increases high-voltage reliability. The detector high-voltage adopts DC high-voltage module and vacuum suction sample board, which improves the angle measurement accuracy and speed. Overall, the X-ray crystal orienter is a precision instrument based on the principle of X-ray diffraction, which provides important technical support for crystal material research and related applications by accurately measuring the cutting angle of crystals.
The TDF series X-ray crystal analyzer is a large-scale analytical instrument and X-ray instrument used to study the internal microstructure of materials. It is mainly used for single crystal orientation, defect inspection, determination of lattice parameters, determination of residual stress, study of the structure of plates and rods, study of the structure of unknown substances, and single crystal dislocations.
The TD-5000 X-ray single crystal diffractometer is mainly used to determine the three-dimensional spatial structure and electron cloud density of crystalline substances such as inorganic, organic, and metal complexes, and to analyze the structure of special materials such as twinning, non commensurate crystals, quasicrystals, etc. Determine the accurate three-dimensional space (including bond length, bond angle, configuration, conformation, and even bonding electron density) of new compound (crystalline) molecules and the actual arrangement of molecules in the lattice; It can provide information on the crystal cell parameters, space group, crystal molecular structure, intermolecular hydrogen bonding and weak interactions, as well as structural information such as molecular configuration and conformation. X-ray single crystal diffractometer is widely used in analytical research in chemical crystallography, molecular biology, pharmacology, mineralogy, and materials science. Single crystal XRD is a high-tech product under the National Major Scientific Instrument and Equipment Development Project of the Ministry of Science and Technology, led by Dandong Tongda Technology Co., Ltd., filling the gap in the development and production of single crystal x-ray diffractometer in China.
The TDF series X-ray crystal analyzer is a large-scale analytical instrument used to study the internal microstructure of substances. It is mainly used for single crystal orientation, defect inspection, determination of lattice parameters, determination of residual stresses, study of the structure of plates and rods, study of the structure of unknown substances, and single crystal dislocations.
The TD-5000 X-ray single crystal diffractometer is mainly used to determine the three-dimensional spatial structure and electron cloud density of crystalline substances such as inorganic, organic, and metal complexes, and to analyze the structure of special materials such as twinning, non commensurate crystals, quasicrystals, etc. Determine the accurate three-dimensional space (including bond length, bond angle, configuration, conformation, and even bonding electron density) of new compound (crystalline) molecules and the actual arrangement of molecules in the lattice; It can provide information on the crystal cell parameters, space group, crystal molecular structure, intermolecular hydrogen bonding and weak interactions, as well as structural information such as molecular configuration and conformation. It is widely used in analytical research in chemical crystallography, molecular biology, pharmacology, mineralogy, and materials science.
Fiber accessories are tested for their unique crystal structure using X-ray diffraction (transmission) method. Test the orientation of the sample based on the fiber crystallinity and half peak width of the fibers. This type of accessory is usually installed on a wide-angle diffractometer and is mainly used to study the texture of thin films on the substrate, perform crystal phase detection, orientation, stress testing, and other tests.
The graphite curved crystal monochromator is installed in front of the X-ray detector, which monochromatizes the X-rays passing through the receiving slit and only detects the K α characteristic X-ray diffractometer accessories of the X-ray spectrum. By using this device, continuous X-rays, K β characteristic X-rays, and fluorescent X-rays can be completely eliminated, enabling high signal-to-noise ratio X-ray diffraction analysis. When copper target X-ray tubes are used in conjunction with corresponding monochromators, fluorescent X-rays generated from Mn, Fe, Co, Ni based samples can be eliminated, making them suitable for analysis of various samples.
The TDF series X-ray crystal analyzer is a large-scale analytical X-ray instrument used to study the internal microstructure of substances.It is mainly used for single crystal orientation,defect inspection,determination of lattice parameters, determination of residual stresses, study of the structure of plates and rods, study of the structure of unknown substances, and single crystal dislocations. The TDF series X-ray crystal analyzer adopts a vertical tube sleeve, and four windows can be used simultaneously. The TDF series X-ray crystal analyzer adopts imported PLC control technology, with high control accuracy and good anti-interference performance, which can achieve reliable operation of the system. The PLC controls the high-voltage switch, lifting, and has the function of automatically training the X-ray tube, effectively extending the service life of the X-ray tube and X-ray instrument.
X-ray single crystal diffractometer is mainly used to determine the three-dimensional spatial structure and electron cloud density of crystalline substances such as inorganic,organic,and metal complexes,and to analyze the structure of special materials such as twinning, non commensurate crystals,quasicrystals,etc.Determine the accurate three-dimensional space (including bond length, bond angle,configuration,conformation,and even bonding electron density) of new compound (crystalline) molecules and the actual arrangement of molecules in the lattice;Single crystal X-ray diffractometer can provide information on the crystal cell parameters,space group,molecular structure,intermolecular hydrogen bonding and weak interactions,as well as structural information such as molecular configuration and conformation.Single crystal XRD is widely used in analytical research in chemical crystallography,molecular biology,pharmacology,mineralogy,and materials science. Single crystal XRD has high precision: 2θ angle repeatability accuracy: 0.0001°; Minimum step angle: 0.0001°; Temperature control range:100K-300K Control accuracy: ±0.3K Single crystal angle measuring instrument selects four concentric scanning circles. Single crystal XRD adopts low-temperature configuration. The company's technical personnel have completed the installation and debugging of the foreign single crystal X-ray diffractometer,and the test results have greatly satisfied foreign users. At the same time,the functionality,stability,and after-sales service of the instrument have received unanimous praise from foreign users. Overall, X-ray single crystal diffractometer plays an irreplaceable role as an important scientific instrument in research and application in multiple disciplines. With the continuous advancement and innovation of technology, we believe that in the future,single crystal XRD will demonstrate their unique value and potential in more fields.
The TDF series X-ray crystal analyzer is a large-scale X-ray instrument used to study the internal microstructure of substances. It utilizes the principle of interaction between X-ray and crystal to determine the atomic arrangement inside the crystal by analyzing the diffraction pattern of X-ray. Mainly used for single crystal orientation, defect inspection, determination of lattice parameters, determination of residual stress, study of the structure of plate and rod, investigation of the structure of unknown substances and single crystal dislocations. The X-ray crystal analyzer, as an X-ray instrument, provides valuable information for materials science research and other related fields. With the continuous advancement of technology and the expansion of applications, X-ray crystal analyzer will continue to play an important role in scientific research and industrial production.