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The high temperature accessory in a diffractometer is an additional device that can perform X-ray diffraction analysis on samples under high temperature conditions. To understand the changes in crystal structure of samples during high-temperature heating and the changes in mutual dissolution of various substances during high-temperature heating. Working principle of high temperature accessory: By using methods such as resistance heating, induction heating, or radiation heating, the sample is heated within a set temperature range. At the same time, it is equipped with high-precision temperature sensors and control systems to monitor and adjust the temperature of the sample in real time, ensuring the stability and accuracy of the temperature. The temperature control accuracy can reach ±0.5℃ or even higher. In order to maintain the stability of the sample at high temperatures and prevent it from reacting with oxygen in the air, high temperature accessory usually require an atmosphere protection system. Common atmospheres include inert gases such as argon, nitrogen, etc. The atmosphere control system can accurately control the flow rate and pressure of the atmosphere, providing a stable experimental environment for the sample. The main functions of high temperature accessory is: Real time monitoring of sample phase transition, chemical reactions, crystal structure changes, and other processes can be carried out in high-temperature environments to obtain information on the structure and properties of substances at different temperatures. By analyzing the position, intensity, and shape of diffraction peaks, the crystal cell parameters, crystal structure, phase composition, and other information of the sample can be obtained, and the content of each component can be accurately measured. Study the rate, mechanism, and diffusion behavior of chemical reactions. For example, observing the structural changes of catalysts during high-temperature reactions, understanding the formation and disappearance of their active centers, and optimizing the performance of catalysts. Application area of high temperature accessory: Used to study the phase transition, crystal structure evolution, and performance changes of high-temperature superconducting materials, metal alloys, ceramic materials, etc. at different temperatures, providing a basis for material design and preparation. Monitoring the changes in substances during chemical reactions, such as studying the structural changes of catalysts and the evolution of active centers in high-temperature catalytic reactions, can help develop efficient catalysts. Study the physical properties of substances at high temperatures, such as magnetism, electronic structure, and their relationship with temperature, and explore new physical phenomena and laws. Technical parameter of high temperature accessory: Temperature setting: Inert gas environment from room temperature to 1200 ℃ Vacuum environment: high temperature of 1600 ℃ Temperature control accuracy: ± 0.5 ℃ Window material: Polyester film Cooling method: deionized water circulation cooling In summary, the high temperature accessory in the diffractometer is an important testing tool that can perform X-ray diffraction analysis on samples under high temperature conditions, providing strong support for research in fields such as materials science, chemical engineering, and physics.
The medium and low temperature accessory of an X-ray diffractometer is a key component used for X-ray diffraction analysis in low-temperature environments.The medium and low temperature accessory is widely used in research and development work in materials science, physics, chemistry, and other fields, especially suitable for scenarios that require structural analysis of materials under different temperature conditions. In order to understand the changes in crystal structure during low-temperature refrigeration process, the following are the technical parameters of the medium and low temperature accessory: Vacuum environment:- 196~500℃ Temperature control accuracy: ± 0.5 ℃ Refrigeration method: liquid nitrogen (consumption less than 4L/h) Window material: Polyester film Cooling method: deionized water circulation cooling In short, the medium and low temperature accessory of X-ray diffractometer is important equipment component that can provide strong support for scientific research and material analysis.The medium and low temperature accessory of a diffractometer is one of the important tools in the field of material structure analysis, with broad application prospects and significant research value.The medium and low temperature accessory of the diffractometer is a key component to ensure the normal operation and accurate measurement of the instrument under low-temperature conditions. Its design and performance directly affect the accuracy and reliability of experimental results. When selecting and applying medium and low temperature accessory, experimental requirements, sample characteristics, as well as the technical parameters and performance characteristics of the accessories should be fully considered to ensure the best experimental results.
The medium and low temperature accessory is designed to understand the changes in crystal structure during the low-temperature refrigeration process.
High temperature accessory are designed to understand the changes in the crystal structure of samples during high-temperature heating, as well as the changes in mutual dissolution of various substances during high-temperature heating.
Medium and low temperature accessory is an experimental device used for testing and analyzing materials or samples within a specific temperature range (usually a medium low temperature environment). The application areas include materials science, chemical engineering, and drug research and development. With the continuous advancement of technology and the increasing demand for applications, it will play a more important role in the future.
High temperature accessory is experimental equipment used for sample analysis in high temperature environment, in order to understand the changes in crystal structure of samples during high temperature heating and the changes in mutual dissolution of various substances during high temperature heating. According to different experimental requirements, different configurations of high temperature attachment can be selected, such as different window materials and reaction chamber designs, to adapt to specific experimental conditions. High temperature attachment is indispensable temperature accessory in laboratory research, which not only improve the efficiency and accuracy of experiments, but also expand the boundaries of scientific research.
The in-situ medium and low temperature accessory is designed to understand the changes in crystal structure during the low-temperature refrigeration process; In order to provide a medium and low temperature (usually below room temperature but not extremely low temperature, such as a range between -100 ℃ and room temperature) sample environment for microscopes and other instruments. Vacuum environment: -196~500℃ Temperature control accuracy: ±0.5℃ Refrigeration method: liquid nitrogen (consumption less than 4L/h) Window material: Polyester film Cooling method: deionized water circulation cooling
High temperature accessory is designed to understand the changes in the crystal structure of samples during high-temperature heating, as well as the changes in mutual dissolution of various substances during high-temperature heating. High-temperature accessory play a crucial role as important experimental and industrial equipment in multiple fields. Its wide range of application fields, precise technical parameters, and diverse product types make high-temperature accessory an indispensable part of scientific research and industrial production. technical parameter Temperature setting: Inert gas environment from room temperature to 1200 ℃ Vacuum environment with high temperature of 1600 ℃ Temperature control accuracy: ± 0.5 ℃ Window material: Polyester film
X-ray diffractometer (XRD) is the use of diffraction principle, accurate phase analysis, qualitative analysis and so on. Today, we will introduce some accessories that can be equipped with XRD instruments.