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What kind of scientific magic does a small platform contain?

The rotating sample holder in an X-ray diffractometer is a key component used for precise adjustment and fixation of the sample position,the sample can rotate within its own plane, which is beneficial for errors caused by coarse grains. For samples with texture and crystallography, rotating sample holder ensures good reproducibility of diffraction intensity and eliminates preferred orientation. Working principle of rotating sample holder: When the X-ray diffractometer is working, high-energy X-rays generated by the X-ray source are irradiated onto the sample fixed on the rotating sample stage. Due to the specific crystal structure and lattice parameters of the sample, X-rays will undergo scattering, absorption, and diffraction phenomena when interacting with the sample, where diffraction phenomena occur according to the requirements of the Bragg equation. The rotating sample holder can rotate at smaller angles according to the setting, allowing the sample to receive X-ray irradiation at different angles, thereby obtaining diffraction patterns at different angles. In this way, the detector can measure the X-ray intensity after sample diffraction and convert it into an electrical signal to be transmitted to the computer for data processing. The main function of the rotating sample holder is: Rotation method: β axis (sample plane) Rotation speed: 1~60RPM Small step width: 0.1 º Operation mode: Constant speed rotation for sample scanning (step, continuous) Advantages of rotating sample holder: The rotating sample holder can improve the accuracy of diffraction data: For samples with irregular powder or particle shapes, the characteristic of preferred orientation is prone to occur during conventional powder sample preparation, resulting in deviations in the distribution of diffraction intensity and affecting the accuracy of diffraction result analysis. Rotating the sample stage can move the sample in a certain form in an appropriate space, eliminating the influence of preferred orientation to a certain extent, thereby improving the accuracy of diffraction data. The rotating sample holder can adapt to various testing needs: able to adapt to different types of X-ray diffraction angle measuring instruments, such as vertical angle measuring instruments, low-power compact powder diffraction equipment, etc., providing convenience for different testing needs. And rotating sample holder can meet the requirements of various samples and testing conditions by adjusting parameters such as speed and steering. The rotating sample holder can expand the instrument's analytical capabilities: New types of rotating sample stages are constantly being developed and applied, such as some sample stages for in-situ electrochemical X-ray diffraction analysis, which can monitor and analyze the changes of materials in different environments or conditions in real time, expanding the analysis capabilities of X-ray diffraction equipment. In summary, the rotating sample holder in X-ray diffractometer is crucial for accurately obtaining crystal structure information of substances. the rotating sample holder can not only improve the accuracy of diffraction data, but also adapt to various testing needs and expand the analytical capabilities of the instrument.

2025/03/14
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The secret weapon of material research

The multi-function sample holder in an X-ray diffractometer is a device used for placing and fixing samples, with multiple functions and features. It can test trace amounts of powder samples, as well as samples that are sheet-like, large-sized, irregular, cannot be cut, or ground into powder. The multi-function sample holder sample fixation and support: The sample holder can firmly fix the sample, ensuring that the sample remains stable during X-ray diffraction and preventing the accuracy and reliability of diffraction data from being affected by sample movement. The multi-function sample holder height and angle adjustment: It has the function of adjusting height and angle, and can flexibly adjust the distance and relative angle between the sample and the X-ray tube and detector according to the size, shape, and detection requirements of different samples, in order to obtain the best diffraction effect. The multi-function sample holder rotation function: Some sample tables can rotate, allowing the sample to receive X-ray irradiation at different angles, thereby obtaining more diffraction information from different angles, which helps to comprehensively analyze the crystal structure and orientation of the sample. The multi-function sample holder adaptation: It can adapt to different types of samples, such as solid, liquid, powder, etc. By replacing different sample fixtures or accessories, it can meet the testing requirements of various samples. The multi-function sample holder environmental control: Some advanced sample holders are also equipped with environmental control systems that can test samples under specific temperature, humidity, atmosphere, and other conditions to simulate the effects of different environments on samples, further expanding the application range of X-ray diffractometers. The multi-function sample holder in X-ray diffractometer is a powerful, flexible and versatile auxiliary equipment, which is of great significance for improving the accuracy and efficiency of X-ray diffraction experiments.

2025/03/11
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Laboratory Innovation

The multi-function sample holder can test trace amounts of powder samples, as well as samples that are sheet-like, large-sized or irregular, cannot be cut or ground into powder.It is an experimental equipment used in scientific research and industrial fields to carry, heat, rotate, and pattern samples, and is an accessory of X-ray diffractometers.

2024/12/12
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Efficient assistant for scientific research and industry

The multi-function sample holder is a device used to provide flexibility and high efficiency in various scientific research and industrial applications. It is commonly used in X-ray diffraction (XRD) analysis and electron microscopy, and is an accessory of X-ray diffractometers (XRD accessory). As an accessory of X-ray diffractometers (XRD accessory) usually equipped with adjustable countertops to accommodate samples of different sizes and shapes.The multi-function sample holder is one of the indispensable tools in modern laboratories and research institutions. It greatly promotes the development of scientific research and industrial applications by providing a flexible, efficient, and accurate sample processing and analysis platform. Whether in the fields of materials science, biomedicine, or electronics industry, multifunction sample holder play an important role in helping researchers and engineers better understand and improve their research subjects.

2024/11/25
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Unlock new experimental skills

Multi-function Sample Holder belongs to the X-ray diffractometer accessory(XRD accessory), which adopts advanced design technology and modular design ideas, and achieves functions such as rotation, lifting differential, and high-temperature oxidation resistance through the combination of different modules. Multi-function Sample Holder is suitable for various advanced thin film growth and deposition technologies, including MBE (molecular beam epitaxy), PLD (pulsed laser deposition), magnetron sputtering, and EB (electron beam evaporation), and can also be used for substrate annealing, high-temperature degassing, and material modification. The substrate of multi-function Sample Holder can reach a maximum heating temperature of 1100 ℃, and can be connected to RF/DC, with self rotation and a speed of 0-20 revolutions per minute. It is continuously adjustable and provides zero positioning. The modular design allows for multiple combination configurations to be selected, and the sample size can accommodate up to 8 inches. In summary, multi-function Sample Holder is a powerful and flexible experimental equipment, suitable for various scientific research and industrial applications as an X-ray diffractometer accessory (XRD accessory). The modular design and multiple functions of the multifunctional sample stage make it an indispensable tool in laboratories and industrial production.

2024/11/13
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Diffractometer accessories

X-ray diffractometer (XRD) is the use of diffraction principle, accurate phase analysis, qualitative analysis and so on. Today, we will introduce some accessories that can be equipped with XRD instruments.

2023/10/05
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Knowledge about "JADE software analysis and processing of XRD data"(三)

Today we share some knowledge about "JADE software analysis and processing XRD data"

2023/08/23
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